jammu university
baba ambedkar university
Total years of experience :1 years, 1 Months
• Qualitative analysis of less common rare metal
Analysis of mixture containing less common metals ion TI, W, Mo, Te, Zr, Ce, Th, U, Li.(Four metal ions in Cationic/anionic forms).
• Separation and estimation of two metals Ions.
Cu-Ni: Estimation of both by gravimetric method.
Ba-Cu: Estimation of Ba gravimetrically and Cu volumetrically.
Ag-Cu, Estimation of Ag gravimetrically and Cu volumetrically.
Cu-Zn: Estimation of both by gravimetric method.
Ni-Zn: Estimation of both by gravimetric method.
Cu-Fe: Estimation of both by gravimetric method.
Ca-Mg: Estimation of both by titrating against EDTA solution.
Zn-Mg: Estimation of both by titrating against EDTA solution.
• To determine the total hardness of water (due to presence of Ca2+ and Mg2+ salts).
• Quantitative Analysis.
Separation, purification and identification of compounds of binary mixture (one liquid and one solid) using TLC and column chromatography, chemical tests, IR separation for functional group identification.
• Organic Synthesis.
Oxidation: Adipic acid by chromic acid oxidation of cyclohexanol.
Grignard reaction: synthesis of triphenylmethanol from benzoic acid.
Aldol condensation: Dibenzal acetone and benzylidene acetone from benzaldehyde.
• Preparation of selected inorganic compounds.
1. Hg \[Co (NCS) 4\], \[Cu (NH3)4\] SO4 H2O, K3 \[Cr (C2O4)3\]. 3H2O etc.
• Structural investigation by I.R, electronic spectra and magnetic susceptibility measurement.
• Preparation of organic inorganic compound and their study by I.R, electronic spectra.
Selection can be made from :-
Sodium amide, Inorg. Synth
Trialkoxyboranes - Preparation, IR and NMR spectra etc.
• Gravimetric and volumetric analysis for Vanadium, Nickel, Mn, Al, Cl.
• Separation, purification, and identification of organic compounds
benzaldehyde. * Preparation of selected inorganic compounds. 1. Hg [Co (NCS) 4], [Cu (NH3)4] SO4 H2O,K3 [Cr (C2O4)3]. 3H2O etc. * Structural investigation by I.R, electronic spectra and magnetic susceptibility measurement. * Preparation of organic inorganic compound and their study by I.R, electronic spectra. Selection can be made from :- Sodium amide, Inorg. Synth Trialkoxyboranes - Preparation, IR and NMR spectra etc. * Gravimetric and volumetric analysis for Vanadium, Nickel, Mn, Al, Cl. * Separation, purification, and identification of organic compounds.
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education
Mechanism * Quantum Chemistry * Organic Reaction Mechanism * Spectroscopy * Bio-organic and Medicinal Chemistry * Organotransition Metal Chemistry. * Solid State chemistry * Group theory & transition metal chemistry. * Chemical Dynamics, Surface and Electro Chemistry * Photochemistry and Spectroscopy in Inorganic Chemistry * Thermodynamics and Statistical Mechanics * Polymer Chemistry * Material Chemistry Page 2 of 3 PROFESSIONAL & PRACTICAL’S SYNOPSIS